Photoisomerization of 1,2-Diphenyl-6-methyl-2,3-dihydro-4-pyridone

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3-Methyl-1,5-diphenyl-4,5-dihydro-1H-pyrazole

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4-Hy­droxy-3-[(4-hy­droxy-6-methyl-2-oxo-3,6-dihydro-2H-pyran-3-yl)(3-thien­yl)meth­yl]-6-methyl-3,6-dihydro-2H-pyran-2-one

The asymmetric unit of the title compound, C(17)H(14)O(6)S, contains four crystallographically independent mol-ecules in which the pyran-one units are essentially planar, with maximum deviations of 0.016 (2), 0.019 (2), 0.025 (2), 0.014 (2), 0.020 (2), 0.010 (2), 0.003 (2) and 0.012 (2) Å. One of the thio-phene rings is disordered over two positions, with an occupancy ratio of 0.739 (4):0.261 (...

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5-Methyl-2-pyridone

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4-(4-Methoxy­phen­yl)-4-methyl-2,6-diphenyl-4H-thio­pyran

The asymmetric unit of the title compound, C(25)H(22)OS, comprises two similar 4-(4-methoxy-phen-yl)-4-methyl-2,6-diphenyl-4H-thio-pyran mol-ecules. In each, the six-membered thio-pyran ring adopts a planar conformation (r.m.s. deviation of 0.041Å for the ring in one mol-ecule and 0.008 Å in the other). The methoxy-phenyl substituent is in a pseudo-axial position. The crystal studied is an inve...

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2-(4-Methoxyphenoxy)-6-methyl-3-oxo-3,6-dihydro-2H-pyran-4-yl benzoate

The title compound, C(20)H(18)O(6), has been synthesized from 4-methoxy-phenyl 3-O-benzo-yloxy-α-l-rhamnopyran-oside by oxidation on treatment with pyridinium dichromate in the presence of acetic anhydride. In the mol-ecule, the pyran ring adopts an envelope conformation with the O atom at the flap position. Weak inter-molecular C-H⋯O hydrogen bonding is present in the crystal structure.

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ژورنال

عنوان ژورنال: Bulletin of the Chemical Society of Japan

سال: 1969

ISSN: 0009-2673,1348-0634

DOI: 10.1246/bcsj.42.3596